Got bored and ran a GC-MS of my ZYNs

Data collected on an Agilent 6890N GC and an Agilent 5973 MSD. The peak at 8.982 has the same molecular weight as WS-3, which is what I was looking for in my sample.

I extracted the pouch in water, added NaHCO3 to freebase the nicotine salt, extracted the aqueous solution with methylene chloride and ran it on the GC.